C₂₆H₃₈ClNO₆

Base Information

Chemical Name:C₂₆H₃₈ClNO₆
CAS No.:1559072-18-2
Molecular Formula:C₂₆H₃₈ClNO₆
Molecular Weight:496.044
Hs Code.:

C<sub>26</sub>H<sub>38</sub>ClNO<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₈ClNO₆

Chemical Property:

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Technology Process of C₂₆H₃₈ClNO₆

There total 5 articles about C₂₆H₃₈ClNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5831-72-1
N-methylpent-4-en-1-amine

: 1559072-10-4
C₂₀H₂₇ClO₇

: 1559072-18-2
C₂₆H₃₈ClNO₆

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 21h;
DOI:10.1039/c3ob42211a

Reference yield:

: 3187-58-4
methyl orsellinate

: 1559072-18-2
C₂₆H₃₈ClNO₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuryl dichloride / tetrahydrofuran / 0.58 h / -30 - -20 °C

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

3.1: potassium hydroxide; water / methanol / 72 h / 70 °C

4.1: sec.-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

4.2: 0.83 h / -78 °C

5.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 21 h / 20 °C

With sulfuryl dichloride; water; sec.-butyllithium; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42211a

Reference yield:

: 1559071-83-8
methyl 3-chloro-4,6-di(ethoxymethoxy)-2-methylbenzoate

: 1559072-18-2
C₂₆H₃₈ClNO₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide; water / methanol / 72 h / 70 °C

2.1: sec.-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

2.2: 0.83 h / -78 °C

3.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 21 h / 20 °C

With water; sec.-butyllithium; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42211a