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chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle

Base Information Edit
  • Chemical Name:chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle
  • CAS No.:711-47-7
  • Molecular Formula:C9H9ClO4
  • Molecular Weight:216.621
  • Hs Code.:
  • Mol file:711-47-7.mol
chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle

Synonyms:chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle

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Chemical Property of chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle Edit
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Technology Process of chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle

There total 6 articles about chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sulfuryl dichloride; In diethyl ether; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2010.04.024
Guidance literature:
methanol; With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 ℃; for 1h; Inert atmosphere;
3-chloro-4,6-dihydroxy-2-methylbenzoic acid; In tetrahydrofuran; toluene; at 0 ℃; for 1.5h;
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium dihydrogenphosphate dihydrate / water; dimethyl sulfoxide / 0.08 h / 0 °C
1.2: 15 h / 0 - 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 0 °C
With sodium dihydrogenphosphate dihydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; dimethyl sulfoxide; toluene;
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