Technology Process of [palladium(II)(2-(diphenylphosphino)-N-[2-(diphenylphosphino)benzylidene]benzeneamine-κ3P,N,P)Cl]BF4
There total 1 articles about [palladium(II)(2-(diphenylphosphino)-N-[2-(diphenylphosphino)benzylidene]benzeneamine-κ3P,N,P)Cl]BF4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
dichloromethane;
Sonication; a mixture of Pd-complex and AgBF4 in dichloromethane exposed to ultrasound for 1 h resulting in precipitates; mixture filtered through kieselguhr and the trapped yellow precipitate dissolved and washed through into the filtrate with CH3CN; filtrate takento dryness in vacuo; crystallized from CH2Cl2/n-hexane; washed with CH2 Cl2/n-pentane; air-dried; elem. anal.;
DOI:10.1016/j.poly.2004.01.015
