[Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3]

Base Information

Chemical Name:[Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3]
CAS No.:1044556-82-2
Molecular Formula:CF₃O₃S*C₃₂H₃₀Fe₃NO₄S
Molecular Weight:841.272
Hs Code.:

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Chemical Property of [Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3]

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Technology Process of [Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3]

There total 1 articles about [Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 912568-30-0
[Fe2(μ-η1:η3-C(Me)=C(S)C=N(Me)(2,6-Me2C6H3))(μ-CO)(CO)(Cp)2]

: 2923-28-6
silver trifluoromethanesulfonate

: 1044556-82-2
[Fe2(μ-η1:η3-Cγ(Me)=Cβ(S-Fe(CO)2(Cp))Cα=N(Me)(Xyl))(μ-CO)(CO)(Cp)2][SO3CF3]

Guidance literature:: In dichloromethane; under N2 atm. to soln. (Fe2(μ-CO)2(CO)2(Cp)2) in CH2Cl2 AgOTf was added and stirred in the dark for 3 h, soln. was filtered through Celite and treated with vinyliminium Fe complex, stirred for 1 h; solvent was removed, chromy. on alumina (MeOH); elem. anal.;
DOI:10.1016/j.jorganchem.2008.04.010