C₂₆H₄₁N₂O₆PSi

Base Information

• Chemical Name: C₂₆H₄₁N₂O₆PSi
• CAS No.: 134937-22-7
• Molecular Formula: C₂₆H₄₁N₂O₆PSi
• Molecular Weight: 536.681
• Mol file: 134937-22-7.mol

Synonyms:

Chemical Property of C₂₆H₄₁N₂O₆PSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₁N₂O₆PSi

There total 1 articles about C₂₆H₄₁N₂O₆PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3,5-dimethoxybenzoate (2150-37-0) + 2-Methyl-5-(tert-butyldimethylsilyloxy)phenyl N,N,N',N'-tetramethylphosphorodiamidate (132552-87-5) → C26H41N2O6PSi (134937-22-7)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction; 1) cyclohexane, THF, -105 deg C, 20 min 2) THF, -105 deg C, 1h;

DOI:10.1248/cpb.39.579

Reference yield: 52.0%

C26H41N2O6PSi (134937-22-7) → 2-(3,5-dimethoxyphenyl)-6-hydroxybenzofuran (134937-20-5)

Guidance literature:

With formic acid; for 1h; Heating;

DOI:10.1248/cpb.39.579

Reference yield:

C26H41N2O6PSi (134937-22-7) → moracin M (56317-21-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / 90percent HCO₂H / 1 h / Heating

2: 18 percent / BBr₃ / CH₂Cl₂ / 480 h / Ambient temperature

With formic acid; boron tribromide; In dichloromethane;

DOI:10.1248/cpb.39.579

upstream raw materials:

methyl 3,5-dimethoxybenzoate

2-Methyl-5-(tert-butyldimethylsilyloxy)phenyl N,N,N',N'-tetramethylphosphorodiamidate

Downstream raw materials:

2-(3,5-dimethoxyphenyl)-6-hydroxybenzofuran

moracin M

6-Hydroxy-2-(3'-hydroxy-5'-methoxyphenyl)benzofuran