Technology Process of C47H50F3N3O5
There total 9 articles about C47H50F3N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
With
oxalyl dichloride; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 6 steps
1: nitric acid; acetic acid / 3 h / 20 °C / Inert atmosphere
2: trichlorophosphate; pyridine / 2 h / Inert atmosphere; Reflux
3: potassium fluoride; 18-crown-6 ether / tetrahydrofuran / 36 h / Reflux; Inert atmosphere
4: 5%-palladium/activated carbon; hydrogen / methanol / 24 h / 760.05 Torr / Inert atmosphere
5: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
6: triethylamine / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
With
pyridine; potassium fluoride; 18-crown-6 ether; 5%-palladium/activated carbon; hydrogen; nitric acid; acetic acid; triethylamine; trichlorophosphate;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201304161
