C₁₈H₁₇ClN₄O

Base Information

Chemical Name:C₁₈H₁₇ClN₄O
CAS No.:1049648-74-9
Molecular Formula:C₁₈H₁₇ClN₄O
Molecular Weight:340.812
Hs Code.:

C<sub>18</sub>H<sub>17</sub>ClN<sub>4</sub>O

Synonyms:

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Chemical Property of C₁₈H₁₇ClN₄O

Chemical Property:

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Technology Process of C₁₈H₁₇ClN₄O

There total 8 articles about C₁₈H₁₇ClN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2457-47-8
3,5-dichloropyridine

: C₁₉H₂₆BN₃O₃

: 1049648-74-9
C₁₈H₁₇ClN₄O

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 120 ℃;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 693774-26-4
(3-bromophenyl)(cyclopropyl)methanone

: 1049648-74-9
C₁₈H₁₇ClN₄O

Guidance literature:: Multi-step reaction with 8 steps

1: potassium cyanide / 120 °C

2: water; potassium hydroxide / 24 h / 185 °C

4: sodium hydrogencarbonate / dichloromethane; water

5: N-ethyl-N,N-diisopropylamine / 70 °C

6: tert.-butylhydroperoxide; ammonium hydroxide

7: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 120 °C

8: potassium carbonate / dimethyl sulfoxide / 120 °C

With tert.-butylhydroperoxide; potassium cyanide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium hydroxide; water; potassium acetate; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane; water; dimethyl sulfoxide; 1: Bucherer-Bergs reaction / 8: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 1049669-09-1
C₁₁H₁₂BrNO₂

: 1049648-74-9
C₁₈H₁₇ClN₄O

Guidance literature:: Multi-step reaction with 6 steps

2: sodium hydrogencarbonate / dichloromethane; water

3: N-ethyl-N,N-diisopropylamine / 70 °C

4: tert.-butylhydroperoxide; ammonium hydroxide

5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 120 °C

6: potassium carbonate / dimethyl sulfoxide / 120 °C

With tert.-butylhydroperoxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium hydroxide; potassium acetate; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; dimethyl sulfoxide; 6: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.013