fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate)

Base Information

Chemical Name:fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate)
CAS No.:858135-74-7
Molecular Formula:C₂₂H₁₇MnN₃O₃*ClO₄
Molecular Weight:525.784
Hs Code.:

fac-[Mn(xylyl isocyanide)(CO)<sub>3</sub>(2,2′-bipyridine)](perchlorate)

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Chemical Property of fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate)

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Technology Process of fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate)

There total 1 articles about fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 38173-71-6
{MnBr(2,2'-bipyridyl)(CO₃)3}

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: silver perchlorate

: 858135-74-7
fac-[Mn(xylyl isocyanide)(CO)₃(2,2′-bipyridine)](perchlorate)

Guidance literature:: In acetone; byproducts: AgBr; (N2); stirring a mixt. of Mn complex and silver salt in acetone for 1 h in the dark, filtration, addn. of isocyanide, stirring for 3 h; evapn., dissolving in CH2Cl2, addn. of hexane, filtration, drying in vac.; elem. anal.;
DOI:10.1021/om700718x