C₃₅H₃₆N₄O₆

Base Information

Chemical Name:C₃₅H₃₆N₄O₆
CAS No.:1591742-00-5
Molecular Formula:C₃₅H₃₆N₄O₆
Molecular Weight:608.694
Hs Code.:

C<sub>35</sub>H<sub>36</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₃₆N₄O₆

Chemical Property:

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Technology Process of C₃₅H₃₆N₄O₆

There total 4 articles about C₃₅H₃₆N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-35-5
acetamide

: 1591741-96-6
C₄₀H₃₈ClN₃O₅

: 1591741-98-8
C₄₂H₄₂N₄O₆

: 1591742-00-5
C₃₅H₃₆N₄O₆

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 20 - 130 ℃; for 1.5h; Overall yield = 127 mg; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ml500077j

Reference yield:

: 918538-05-3
2,4-dichloro-pyrrolo[2,1-f][1,2,4]triazine

: 1591741-98-8
C₄₂H₄₂N₄O₆

: 1591742-00-5
C₃₅H₃₆N₄O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / -10 - 20 °C

1.2: 3 h / -10 - 20 °C

2.1: N-Bromosuccinimide / dichloromethane / -10 - 20 °C

2.2: 0.58 h / -100 - -95 °C

3.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

4.1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 1.5 h / 20 - 130 °C / Inert atmosphere; Microwave irradiation

With triethylsilane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; n-butyllithium; boron trifluoride diethyl etherate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/ml500077j

Reference yield:

: 1591741-85-3
C₁₃H₁₀ClN₃O

: 1591741-98-8
C₄₂H₄₂N₄O₆

: 1591742-00-5
C₃₅H₃₆N₄O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / -10 - 20 °C

1.2: 0.58 h / -100 - -95 °C

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

3.1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 1.5 h / 20 - 130 °C / Inert atmosphere; Microwave irradiation

With triethylsilane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; boron trifluoride diethyl etherate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ml500077j