di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride

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Chemical Name:di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride
CAS No.:1346678-81-6
Molecular Formula:C₈₈H₅₆ClF₁₈N₁₀P₂Ru₂*Cl
Molecular Weight:1930.44
Hs Code.:

di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride

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Chemical Property of di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride

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Technology Process of di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride

There total 1 articles about di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 960594-76-7
2,6-bis(5-diphenyl-1H-pyrazol-3-yl)pyridine

: 14898-67-0
ruthenium(III) chloride trihydrate

: 13406-29-6
tris(para-trifluoromethyl)phenyl phosphine

: 1346678-81-6
di[(2-(5-phenyl-1H-pyrazol-3-yl)-6-(5-phenylpyrazol-3-yl)pyridine)(tri(p-trifluoromethylphenyl)phosphine)ruthenium(II)](μ-chloro) chloride

Guidance literature:: With Et₃N; In ethanol; (N2), RuCl3*3H2O and ligand (1:1.1) refluxed in EtOH for 5 h, cooled to room temp., filtered, washed (EtOH/Et2O), dried (vac.), suspnd. in EtOH,treated with 1 equiv. of ligand and excess of Etg3N, refluxed for 6 h; cooled to room temp., evapd.(vac.), extd.(Et2O), filtered, concd.(vac.),layered (n-hexane), diffused into Et2O soln. over 24 h, filtered, dried (vac.), elem. anal.;
DOI:10.1016/j.inoche.2011.09.003