C₃₈H₃₅BrN₂O₇

Base Information

Chemical Name:C₃₈H₃₅BrN₂O₇
CAS No.:1234550-83-4
Molecular Formula:C₃₈H₃₅BrN₂O₇
Molecular Weight:711.609
Hs Code.:

C<sub>38</sub>H<sub>35</sub>BrN<sub>2</sub>O<sub>7</sub>

Synonyms:

Suppliers and Price of C₃₈H₃₅BrN₂O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₈H₃₅BrN₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₈H₃₅BrN₂O₇

There total 27 articles about C₃₈H₃₅BrN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1150635-60-1
C₂₂H₂₅NO₇

: 1234550-83-4
C₃₈H₃₅BrN₂O₇

Guidance literature:: Multi-step reaction with 21 steps

1.1: methanol; potassium carbonate / 1 h / 0 °C / Inert atmosphere

1.2: 0 °C / pH 3

2.1: 10% palladium on activated carbon; hydrogen / methanol / 10 h / 20 °C / 760.05 Torr

3.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

5.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

6.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

8.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

9.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

9.2: 0 °C

10.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

11.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

12.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

13.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

14.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

15.1: 3,3-dimethyldioxirane / methanol; acetone / 2 h / 0 °C / Inert atmosphere

16.1: CSA / 0 - 20 °C / Inert atmosphere

17.1: sodium cyanoborohydride; trifluoroacetic acid / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

18.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

19.1: toluene-4-sulfonic acid / methanol / 5 h / Inert atmosphere; Reflux

20.1: potassium trimethylsilonate / acetonitrile / 2.5 h / 0 - 50 °C / Inert atmosphere

20.2: 0 °C

21.1: hydrogenchloride; water / 1,4-dioxane / 4 h / 0 - 95 °C

With hydrogenchloride; methanol; N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; 10% palladium on activated carbon; potassium trimethylsilonate; water; hydrogen; 3,3-dimethyldioxirane; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium cyanoborohydride; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetyl chloride; trifluoroacetic acid; potassium iodide; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 13.1: Friedel Crafts alkylation / 21.1: Pomeranz-Fritsch reaction;
DOI:10.1021/jo100788j

Reference yield:

: 1177255-35-4
(S)-methyl 3-(2-bromo-5-hydroxy-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoate

: 1234550-83-4
C₃₈H₃₅BrN₂O₇

Guidance literature:: Multi-step reaction with 18 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

5.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

6.2: 0 °C

7.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

8.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

9.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

10.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

11.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

12.1: 3,3-dimethyldioxirane / methanol; acetone / 2 h / 0 °C / Inert atmosphere

13.1: CSA / 0 - 20 °C / Inert atmosphere

14.1: sodium cyanoborohydride; trifluoroacetic acid / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

15.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

16.1: toluene-4-sulfonic acid / methanol / 5 h / Inert atmosphere; Reflux

17.1: potassium trimethylsilonate / acetonitrile / 2.5 h / 0 - 50 °C / Inert atmosphere

17.2: 0 °C

18.1: hydrogenchloride; water / 1,4-dioxane / 4 h / 0 - 95 °C

With hydrogenchloride; methanol; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; potassium trimethylsilonate; water; 3,3-dimethyldioxirane; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium cyanoborohydride; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetyl chloride; trifluoroacetic acid; potassium iodide; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 10.1: Friedel Crafts alkylation / 18.1: Pomeranz-Fritsch reaction;
DOI:10.1021/jo100788j

Reference yield:

: 1234550-76-5
(R)-tert-butyl 2-(benzyloxy)-1-(6-(methoxymethoxy)-7-methylbenzo[d][1,3]dioxol-4-yl)ethylcarbamate

: 1234550-83-4
C₃₈H₃₅BrN₂O₇

Guidance literature:: Multi-step reaction with 15 steps

1.1: hydrogenchloride; water / 1,4-dioxane; methanol / 5 h / 0 - 20 °C

2.1: sodium hydrogencarbonate / dichloromethane; water / 3 h / 0 - 20 °C / pH 8

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

4.2: 0 °C / pH 8

5.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

6.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

7.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

8.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

9.1: 3,3-dimethyldioxirane / methanol; acetone / 2 h / 0 °C / Inert atmosphere

10.1: CSA / 0 - 20 °C / Inert atmosphere

11.1: sodium cyanoborohydride; trifluoroacetic acid / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

12.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

13.1: toluene-4-sulfonic acid / methanol / 5 h / Inert atmosphere; Reflux

14.1: potassium trimethylsilonate / acetonitrile / 2.5 h / 0 - 50 °C / Inert atmosphere

14.2: 0 °C

15.1: hydrogenchloride; water / 1,4-dioxane / 4 h / 0 - 95 °C

With hydrogenchloride; potassium trimethylsilonate; water; 3,3-dimethyldioxirane; phenyltrimethylammonium tribromide; sodium cyanoborohydride; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 7.1: Friedel Crafts alkylation / 15.1: Pomeranz-Fritsch reaction;
DOI:10.1021/jo100788j