C₂₈H₂₂O₂

Base Information

Chemical Name:C₂₈H₂₂O₂
CAS No.:1370643-07-4
Molecular Formula:C₂₈H₂₂O₂
Molecular Weight:390.481
Hs Code.:

C<sub>28</sub>H<sub>22</sub>O<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₂O₂

Chemical Property:

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Technology Process of C₂₈H₂₂O₂

There total 7 articles about C₂₈H₂₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1370643-06-3
4H-5,6-dihydroanthraceno[9,1-bc]pyran-6-ol-2-one

: 100-58-3
phenylmagnesium bromide

: 1370643-07-4
C₂₈H₂₂O₂

Guidance literature:: 4H-5,6-dihydroanthraceno[9,1-bc]pyran-6-ol-2-one; In diethyl ether; at 20 ℃; for 0.25h;

phenylmagnesium bromide; With hydrogenchloride; water;
DOI:10.1021/jo3003216

Reference yield:

: 90-15-3
α-naphthol

: 1370643-07-4
C₂₈H₂₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1: sulfuric acid / 2.5 h / 0 °C

2: sodium hydride / dimethyl sulfoxide; mineral oil / 0.08 h

3: sodium hydroxide / ethanol / 2 h / Reflux

4: dimethyl sulfoxide / 0.17 h / Reflux

5: thionyl chloride / 1 h / 20 °C / Reflux

6: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

7: sodium tetrahydroborate / ethanol / 1 h / 20 °C

8: diethyl ether / 0.25 h / 20 °C

With aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; sulfuric acid; sodium hydride; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/jo3003216

Reference yield:

: C₁₇H₁₂O₆

: 1370643-07-4
C₂₈H₂₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / 0.17 h / Reflux

2: thionyl chloride / 1 h / 20 °C / Reflux

3: aluminum (III) chloride / dichloromethane / 2 h / 20 °C

4: sodium tetrahydroborate / ethanol / 1 h / 20 °C

5: diethyl ether / 0.25 h / 20 °C

With aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jo3003216