5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

Base Information

Chemical Name:5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone
CAS No.:149220-91-7
Molecular Formula:C₂₉H₂₅NO₅
Molecular Weight:467.521
Hs Code.:

Synonyms:

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Chemical Property of 5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

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Technology Process of 5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

There total 9 articles about 5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 149220-91-7
5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

Guidance literature:: Multi-step reaction with 7 steps

1: 58 percent / Et₃N / dimethylformamide / 15 h / Ambient temperature

2: 90 percent / 1 N aq. NaOH / ethanol / 2 h / 50 °C

3: 64 percent / diethyl cyanophosphate / dimethylformamide / 16 h / Ambient temperature

4: 1.) t-BuLi, 2.) CuCN, 3.) O₂

5: 4 N aq. HCl / ethanol / 0.17 h / 45 °C

6: K₂CO₃ / propan-2-ol / 3 h / Heating

7: 1.) POCl₃, 2.) aq. HCl / 1.) reflux, 10 min, 2.) EtOH, 60 deg C, 30 min

With hydrogenchloride; sodium hydroxide; diethyl cyanophosphonate; tert.-butyl lithium; oxygen; potassium carbonate; triethylamine; trichlorophosphate; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1248/cpb.41.445

Reference yield:

: 149220-87-1
3,4-bis(methoxymethoxy)benzoic acid

: 149220-91-7
5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / diethyl cyanophosphate / dimethylformamide / 16 h / Ambient temperature

2: 1.) t-BuLi, 2.) CuCN, 3.) O₂

3: 4 N aq. HCl / ethanol / 0.17 h / 45 °C

4: K₂CO₃ / propan-2-ol / 3 h / Heating

5: 1.) POCl₃, 2.) aq. HCl / 1.) reflux, 10 min, 2.) EtOH, 60 deg C, 30 min

With hydrogenchloride; diethyl cyanophosphonate; tert.-butyl lithium; oxygen; potassium carbonate; trichlorophosphate; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1248/cpb.41.445

Reference yield:

: 149220-93-9
3,4-bis(methoxymethoxy)-N,N-diethylbenzamide

: 149220-91-7
5,6-dibenzyloxy-1,3-dimethoxy-9(10H)-acridone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) t-BuLi, 2.) CuCN, 3.) O₂

2: 4 N aq. HCl / ethanol / 0.17 h / 45 °C

3: K₂CO₃ / propan-2-ol / 3 h / Heating

4: 1.) POCl₃, 2.) aq. HCl / 1.) reflux, 10 min, 2.) EtOH, 60 deg C, 30 min

With hydrogenchloride; tert.-butyl lithium; oxygen; potassium carbonate; trichlorophosphate; In ethanol; isopropyl alcohol;
DOI:10.1248/cpb.41.445