(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

Base Information

Chemical Name:(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2
CAS No.:120204-95-7
Molecular Formula:C₇H₁₈Cl₂N₇Ru*2ClO₄
Molecular Weight:571.144
Hs Code.:

(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO<sub>4</sub>)2

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Chemical Property of (pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

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Technology Process of (pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

There total 2 articles about (pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: {Ru(NH₃)5(Cl)}⁽²⁺⁾*2PF₆^(1-)={Ru(NH₃)5(Cl)}(PF₆)2

: 120204-98-0
thallium 2,3-dichlorophenylcyanamidate

: 56-34-8
tetraethylammonium chloride

: sodium perchlorate

: 120204-95-7
(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

Guidance literature:: In water; acetonitrile; byproducts: TlCl; addn. of Tl-comp. to soln. of Ru-complex, stirring (45°C, 16 h), TlCl ppt. filtered off, addn. of Et4NCl, pptn., washing (MeCN), chromy. (Sephadex, aq. NaCl), addn. of NaClO4 (pptn.); washing with ice-cold water, recrystn. (ether diffusion into acetone soln.) drying (78°C, vac.); elem. anal.;

Reference yield:

: {Ru(NH₃)5(Cl)}⁽²⁺⁾*2PF₆^(1-)={Ru(NH₃)5(Cl)}(PF₆)2

: 120204-98-0
thallium 2,3-dichlorophenylcyanamidate

: 120204-95-7
(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

Guidance literature:: In not given;

Reference yield: 32.0%

: 120204-95-7
(pentaammineruthenium(III) 2,3-dichlorophenylcyanamide)(ClO₄)2

: sodium perchlorate

: {Ru(NH₃)5((2,3-dichlorophenyl)cyanamide)}(ClO₄)3*1.5H₂O

Guidance literature:: With HClO₄; In water; mixing of solns. of Ru-complex and HClO4 (ice-cooling), addn. of NaClO4, cooling (ice bath, 1 h); ppt. filtered off (succion filtration), washed with aq. HClO4 and ether and forced out from dry acetonitrile soln. by addn. of anhyd. ether; elem. anal.;