2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

Base Information

Chemical Name:2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate
CAS No.:1355333-52-6
Molecular Formula:C₂₂H₁₄O₁₁
Molecular Weight:454.347
Hs Code.:

Synonyms:

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Chemical Property of 2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

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Technology Process of 2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

There total 4 articles about 2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 475161-97-8
benzyl 3,4,5-tris(benzyloxy)benzoate

: 1355333-52-6
2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / 1,4-dioxane; methanol; water / 14 h / Reflux

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 25 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane; ethyl acetate / 16 h / 25 °C / 1861.78 Torr

With dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.bmcl.2011.10.119

Reference yield:

: 117-39-5,74893-81-5
quercetol

: 1355333-52-6
2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / N,N-dimethyl-formamide / 20 h / 80 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 25 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane; ethyl acetate / 16 h / 25 °C / 1861.78 Torr

With dmap; palladium 10% on activated carbon; hydrogen; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.119

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 1355333-52-6
2-hydroxy-5-(3,5,7-trihydroxy-4-oxo-4H-chromen-2-yl)phenyl 3,4,5-trihydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / N,N-dimethyl-formamide / 14 h / 25 °C / Inert atmosphere

2: sodium hydroxide / 1,4-dioxane; methanol; water / 14 h / Reflux

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 25 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane; ethyl acetate / 16 h / 25 °C / 1861.78 Torr

With dmap; palladium 10% on activated carbon; hydrogen; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.119