5-triazole isophthalic acid

Base Information

• Chemical Name: 5-triazole isophthalic acid
• CAS No.: 1184873-47-9
• Molecular Formula: C₁₀H₇N₃O₄
• Molecular Weight: 233.183
• Mol file: 1184873-47-9.mol

Synonyms:

Chemical Property of 5-triazole isophthalic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 5-triazole isophthalic acid

There total 1 articles about 5-triazole isophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

5-aminoisophthalic acid (99-31-0) + {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride} (16227-06-8) → 5-triazole isophthalic acid (1184873-47-9)

Guidance literature:

In benzene; for 8h; Reflux;

DOI:10.1039/c2cc31527k

Reference yield: 37.0%

copper(l) iodide (7681-65-4) + N,N-dimethyl acetamide (127-19-5,116057-81-9) + 5-triazole isophthalic acid (1184873-47-9) + water (7732-18-5) → Cu(2+)*C10H5N3O4(2-)*1.5H2O*C4H9NO

Guidance literature:

at 85 ℃; for 24h;

DOI:10.1002/chem.201505107

Reference yield: 32.0%

copper(l) iodide (7681-65-4) + 5-triazole isophthalic acid (1184873-47-9) + water (7732-18-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → Cu(2+)*C10H5N3O4(2-)*C3H7NO*1.5H2O

Guidance literature:

at 85 ℃; for 24h;

DOI:10.1002/chem.201505107

upstream raw materials:

5-aminoisophthalic acid

{N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride}