Technology Process of 1-(3-Chloropropyl)-2,3,4,5,6-pentamethylbenzene
There total 8 articles about 1-(3-Chloropropyl)-2,3,4,5,6-pentamethylbenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; zinc(II) chloride;
at 130 ℃;
for 14h;
high pressure;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: dimethylsulfoxide / 5 h / 130 °C / high pressure
2: H2SO4, H2O / 10 h / 130 °C
3: 69 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
4: HCl, ZnCl2 / 14 h / 130 °C / high pressure
5: 87 percent / dimethylsulfoxide; H2O / 4 h / 130 °C / high pressure
6: 80 percent / 45percent H2SO4 / 14 h / 130 °C / high pressure
7: 80 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
8: 47 percent / HCl, ZnCl2 / 14 h / 130 °C / high pressure
With
hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; water; zinc(II) chloride;
In
tetrahydrofuran; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 69 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
2: HCl, ZnCl2 / 14 h / 130 °C / high pressure
3: 87 percent / dimethylsulfoxide; H2O / 4 h / 130 °C / high pressure
4: 80 percent / 45percent H2SO4 / 14 h / 130 °C / high pressure
5: 80 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
6: 47 percent / HCl, ZnCl2 / 14 h / 130 °C / high pressure
With
hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; zinc(II) chloride;
In
tetrahydrofuran; water; dimethyl sulfoxide;
