[4-(2-hydroxyethoxy)phenyl]arsonic acid

Base Information

• Chemical Name: [4-(2-hydroxyethoxy)phenyl]arsonic acid
• CAS No.: 5430-34-2
• Molecular Formula: C8H11 As O5
• Molecular Weight: 262.094
• Mol file: 5430-34-2.mol

Synonyms:Benzenearsonicacid, p-b-hydroxyethoxy- (3CI); NSC 13775

Chemical Property of [4-(2-hydroxyethoxy)phenyl]arsonic acid

Chemical Property:

• Vapor Pressure: 8.66E-13mmHg at 25°C
• Boiling Point: 546.8°C at 760 mmHg
• Flash Point: 222.1°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [4-(2-hydroxyethoxy)phenyl]arsonic acid

There total 2 articles about [4-(2-hydroxyethoxy)phenyl]arsonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxyphenylarsonic acid (98-14-6) + 2-chloro-ethanol (107-07-3) → [4-(2-hydroxy-ethoxy)-phenyl]-arsonic acid (5430-34-2)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01326a058

Reference yield:

4-acetaminophenol (103-90-2,8055-08-1) + 2-chloro-ethanol (107-07-3) → [4-(2-hydroxy-ethoxy)-phenyl]-arsonic acid (5430-34-2)

Guidance literature:

With sodium hydroxide; beim Erhitzen des Reaktionsprodukts mit wss.Salzsaeure und Behandeln der aus dem erhaltenen Amin bereiteten Diazoniumsalz-Loesung mit Natriumarsenit;

Reference yield:

[4-(2-hydroxy-ethoxy)-phenyl]-arsonic acid (5430-34-2) → 2-(4-arsenoso-phenoxy)-ethanol (5411-06-3)

Guidance literature:

With hydrogenchloride; sulfur dioxide; hydrogen iodide; und Behandeln des Reaktionsprodukts mit wss.Alkalilauge;

DOI:10.1021/ja01326a058 DOI:10.1021/ja01868a033

upstream raw materials:

4-acetaminophenol

2-chloro-ethanol

4-hydroxyphenylarsonic acid

Downstream raw materials:

2-(4-arsenoso-phenoxy)-ethanol

(4-hydroxy-3,5-dinitro-phenyl)-arsonic acid

[4-(2-hydroxy-ethoxy)-3,5-dinitro-phenyl]-arsonic acid

(4-arsono-2-nitro-phenoxy)-acetic acid