Technology Process of benzo[m]tetraphen-3-ol
There total 7 articles about benzo[m]tetraphen-3-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen bromide;
In
acetic acid;
for 3.5h;
Heating;
DOI:10.1021/jm00402a009
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) sec-butyllithium, TMEDA / 2) THF, -78 deg C (3 h), room temperature, overnight;
2: p-toluenesulfonic acid / benzene / 5 h / Heating
3: 92 percent / Zn, aq. KOH / pyridine / Heating
4: 93 percent / ZnCl2 / acetic acid / 1 h / Heating
5: 100 percent / aq. HI, aq. hypophosphorous acid / acetic acid / 0.03 h / 100 °C
6: 100 percent / HBr / acetic acid / 3.5 h / Heating
With
potassium hydroxide; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; hydrogen iodide; sec.-butyllithium; hypophosphorous acid; toluene-4-sulfonic acid; zinc(II) chloride; zinc;
In
pyridine; acetic acid; benzene;
DOI:10.1021/jm00402a009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / ZnCl2 / acetic acid / 1 h / Heating
2: 100 percent / aq. HI, aq. hypophosphorous acid / acetic acid / 0.03 h / 100 °C
3: 100 percent / HBr / acetic acid / 3.5 h / Heating
With
hydrogen bromide; hydrogen iodide; hypophosphorous acid; zinc(II) chloride;
In
acetic acid;
DOI:10.1021/jm00402a009