((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)

Base Information

Chemical Name:((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)
CAS No.:1221069-43-7
Molecular Formula:C₄₃H₆₅Cl₃N₉OY
Molecular Weight:919.314
Hs Code.:

((CH<sub>3</sub>)2CHNHCNCH(CH<sub>3</sub>)2(NC<sub>6</sub>H<sub>4</sub>Cl))3Y(C<sub>4</sub>H<sub>8</sub>O)

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Chemical Property of ((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)

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Technology Process of ((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)

There total 1 articles about ((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 109-72-8,29786-93-4
n-butyllithium

: 10361-92-9,61894-01-7
yttrium(III) chloride

: 106-47-8
4-chloro-aniline

: 693-13-0
diisopropyl-carbodiimide

: 1221069-43-7
((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)

Guidance literature:: In tetrahydrofuran; hexane; std. Schlenk tech., under Ar; charged with NH2-compd., THF, cooled to 0°C, BuLi in hexane added, warmed to room temp., stirred for 1 h, diimide added at 0°C, warmed to room temp., stirred for 1 h, addedto YCl3 in THF, stirred for 24 h; evapd. to dryness in vac., extracted with Et2O, centrifugated, concentrated, cooled to 0°C, crystallized from ether, elem. anal.;
DOI:10.1016/j.jorganchem.2009.12.010

Reference yield: 62.0%

: 109-72-8,29786-93-4
n-butyllithium

: 110-71-4
1,2-dimethoxyethane

: 1221069-43-7
((CH₃)2CHNHCNCH(CH₃)2(NC₆H₄Cl))3Y(C₄H₈O)

: (((CH₃)2CHN)2CNC₆H₄Cl)3Y^(3-)*3Li⁽¹⁺⁾*3C₄H₈O*3(CH₃OCH₂)2=((((CH₃)2CHN)2CNC₆H₄Cl)3Y)(Li)3*3C₄H₈O*3(CH₃OCH₂)2

Guidance literature:: In tetrahydrofuran; hexane; Schlenk flask charged with Y-compd., THF and a stir bar, cooled to 0°C, BuLi in hexane added, slowly warmed to room temp., stirred for 24h; evapd. to dryness in vac., crystallized from DME and toluene, elem. anal.;
DOI:10.1016/j.jorganchem.2009.12.010