3-chloro-N-cyclohexyl-2-methylenehexanamide

Base Information

Chemical Name:3-chloro-N-cyclohexyl-2-methylenehexanamide
CAS No.:86918-26-5
Molecular Formula:C₁₃H₂₂ClNO
Molecular Weight:243.777
Hs Code.:

Synonyms:

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Chemical Property of 3-chloro-N-cyclohexyl-2-methylenehexanamide

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Technology Process of 3-chloro-N-cyclohexyl-2-methylenehexanamide

There total 4 articles about 3-chloro-N-cyclohexyl-2-methylenehexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 86918-26-5
3-chloro-N-cyclohexyl-2-methylenehexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / triethylamine / diethyl ether / -78 °C

3: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min

4: 1.) n-butyl-lithium, 2.) toluene-4-sulphonyl chloride / 1.) THF, -78 deg C -> 0 deg C, 2.) -78 deg C -> room temperature

With n-butyllithium; triethylamine; p-toluenesulfonyl chloride; In diethyl ether;

Reference yield:

: 5525-85-9
N-Cyclohexylbrenztraubensaeure-amid

: 86918-26-5
3-chloro-N-cyclohexyl-2-methylenehexanamide

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min

3: 1.) n-butyl-lithium, 2.) toluene-4-sulphonyl chloride / 1.) THF, -78 deg C -> 0 deg C, 2.) -78 deg C -> room temperature

With n-butyllithium; p-toluenesulfonyl chloride;

Reference yield:

: 78257-87-1
N-cyclohexyl-2-oxopropanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

: 86918-26-5
3-chloro-N-cyclohexyl-2-methylenehexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min

2: 1.) n-butyl-lithium, 2.) toluene-4-sulphonyl chloride / 1.) THF, -78 deg C -> 0 deg C, 2.) -78 deg C -> room temperature

With n-butyllithium; p-toluenesulfonyl chloride;