cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)

Base Information

Chemical Name:cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)
CAS No.:879280-57-6
Molecular Formula:C₂₅H₂₈B₂P₄
Molecular Weight:474.014
Hs Code.:

cyclo-1,4-(BH<sub>3</sub>)2(P<sub>4</sub>Ph<sub>4</sub>CH<sub>2</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)

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Technology Process of cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)

There total 1 articles about cyclo-1,4-(BH₃)2(P₄Ph₄CH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 13292-87-0
dimethyl sulfide borane

: 40425-94-3,63357-22-2,879280-62-3,879280-63-4,879280-64-5
1,2,3,4-tetraphenylcyclo-5-carba-1,2,3,4-tetraphosphine

: 879713-22-1,879713-24-3,879280-57-6,879713-20-9
cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)

Guidance literature:: In toluene; byproducts: S(CH3)2; (Ar); B compd. (2 equiv.) was added to soln. of P4Ph4CH2 in toluene; soln. was refluxed briefly and stirred overnight; hexane quickly added; stored at room temp. for few d; dried (vac.); elem. anal.;
DOI:10.1039/b511833f

Reference yield:

: 879713-22-1,879713-24-3,879280-57-6,879713-20-9
cyclo-1,4-(BH₃)2(P₄Ph₄CH₂)

: 920-36-5,90269-51-5
(2-methylpropyl)lithium

: 879280-58-7
cyclo-1,4-(BH₃)2(P₄Ph₄CHLi)

Guidance literature:: In hexane; pentane; byproducts: (CH3)2CHCH3; (Ar); soln. of BuLi in hexane was added to soln. of B-P compd. in pentane; mixt. was refluxed for 3.5 h; filtered; dried (vac.);
DOI:10.1039/b511833f