Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3

Base Information

• Chemical Name: Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3
• CAS No.: 700875-40-7
• Molecular Formula: C₃₃H₅₀FeN₂O
• Molecular Weight: 546.62
• Mol file: 700875-40-7.mol

Synonyms:

Chemical Property of Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3

There total 1 articles about Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

((2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FeCl)2 (700875-27-0) + lithium tert-butoxide (1907-33-1) → Fe((CH(CH3)2)2C6H3NCCH3)2CHOC(CH3)3 (700875-40-7)

Guidance literature:

In toluene; Fe-complex was mixed with Li-salt, toluene was added, stirred for 12 h under N2; dried under vac., extd. with pentane, filtered, concd., hexamethyldisiloxane was added, cooled to -35°C; elem. anal.;

DOI:10.1021/ic035483x

Reference yield: 69.0%

Fe((CH(CH3)2)2C6H3NCCH3)2CHOC(CH3)3 (700875-40-7) + silver trifluoromethanesulfonate (2923-28-6) → Fe((CH(CH3)2)2C6H3NCCH3)2CHOC(CH3)3CF3SO3 (700875-43-0)

Guidance literature:

In diethyl ether; Fe-complex was dissolved in Et2O, AgOTf was added, stirred for 2 h underN2; dried under vac., extd. with pentane, concd., cooled at -35°C; elem. anal.;

DOI:10.1021/ic035483x

upstream raw materials:

((2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FeCl)2

lithium tert-butoxide

Downstream raw materials:

Fe((CH(CH₃)2)2C₆H₃NCCH₃)2CHOC(CH₃)3CF₃SO₃