tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

Base Information

Chemical Name:tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)
CAS No.:1221070-18-3
Molecular Formula:C₈H₂₀N*C₂₄H₂₂N₃NiO₄
Molecular Weight:605.4
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

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Technology Process of tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

There total 2 articles about tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: acetonitrile-N,N’-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido-nickel(II)

: 56-34-8
tetraethylammonium chloride

: 590-29-4
potassium formate

: 1221070-18-3
tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

Guidance literature:: In methanol; for 0.166667h;
DOI:10.1002/chem.201704618

Reference yield: 58.0%

: 1221070-09-2
(Et₄N)[Ni(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamidate^(2-))(OH)]

: 109-94-4
formic acid ethyl ester

: 1221070-18-3
tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

Guidance literature:: In dimethylformamide; (N2) soln. Ni complex in DMF was layered with ethyl formate, 2 days; elem. anal.;
DOI:10.1021/ja1003125

Reference yield:

: 1221070-18-3
tetraethylammonium formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickelate(II)

: formato(N,N'-bis(2,6-dimethylphenyl)-2,6-pyridinedicarboxamido)nickel(III)

Guidance literature:: With tris(p-bromophenylammoniumyl) hexachloroantimonate; In acetone; acetonitrile; at -80 ℃; Electrochemical reaction;
DOI:10.1002/chem.201704618