Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester

Base Information

• Chemical Name: Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester
• CAS No.: 100253-12-1
• Molecular Formula: C₁₂H₁₆NO₃PS
• Molecular Weight: 285.304
• Mol file: 100253-12-1.mol

Synonyms:

Chemical Property of Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester

There total 1 articles about Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(I) cyanide (544-92-3) + benzaldehyde (100-52-7) + diethyl phosphorochloridothioate (2524-04-1) → Thiophosphoric acid O-(cyano-phenyl-methyl) ester O',O''-diethyl ester (100253-12-1)

Guidance literature:

With tetrabutyl-ammonium chloride; dmap; Yield given. Multistep reaction; 1.) CH₂Cl₂, 25 deg C; 2.) CH₂Cl₂, H₂O;

DOI:10.1016/S0040-4020(01)87516-5

upstream raw materials:

copper(I) cyanide

benzaldehyde

diethyl phosphorochloridothioate

Refernces