Technology Process of Benzoic acid 13-hydroxy-tridecyl ester
There total 1 articles about Benzoic acid 13-hydroxy-tridecyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: PCC, AcONa / CH2Cl2 / 2 h / Ambient temperature
2: 48 percent / 4 Angstroem MS / toluene / 2 h / Ambient temperature
3: 31 percent / toluene / 48 h
4: 82 percent / DIPEA / CH2Cl2 / 30 h / Heating
5: pyridine / 2 h / 0 °C
6: 77 percent / H2 / Pd(OH)2/C / methanol / 15 h / Ambient temperature
7: tetrahydrofuran / 4 h / Heating
8: Bu3SnH / toluene / 5 h / Heating
With
4 Angstroem MS; hydrogen; tri-n-butyl-tin hydride; sodium acetate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate;
palladium dihydroxide;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4020(98)01012-6
- Guidance literature:
-
Multi-step reaction with 7 steps
1: PCC, AcONa / CH2Cl2 / 2 h / Ambient temperature
2: 48 percent / 4 Angstroem MS / toluene / 2 h / Ambient temperature
3: 31 percent / toluene / 48 h
4: 82 percent / DIPEA / CH2Cl2 / 30 h / Heating
5: pyridine / 2 h / 0 °C
6: 77 percent / H2 / Pd(OH)2/C / methanol / 15 h / Ambient temperature
7: tetrahydrofuran / 4 h / Heating
With
4 Angstroem MS; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate;
palladium dihydroxide;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4020(98)01012-6
