Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)⁽¹⁺⁾*BF₄^(1-)=Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)BF₄

Base Information

• Chemical Name: Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)⁽¹⁺⁾*BF₄^(1-)=Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)BF₄
• CAS No.: 912311-39-8
• Molecular Formula: BF₄*C₃₅H₃₈IrSb₂
• Molecular Weight: 981.211
• Mol file: 912311-39-8.mol

Synonyms:

Chemical Property of Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)⁽¹⁺⁾*BF₄^(1-)=Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)⁽¹⁺⁾*BF₄^(1-)=Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)BF₄

There total 1 articles about Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)⁽¹⁺⁾*BF₄^(1-)=Ir(C₈H₁₂)((C₆H₅)4Sb₂(CH₂)3)BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

silver tetrafluoroborate (14104-20-2) + bis(1,5-cyclooctadiene)diiridium(I) dichloride (12112-67-3) + 1,3-bis(diphenylstibino)propane (38611-86-8) → Ir(C8H12)((C6H5)4Sb2(CH2)3)(1+)*BF4(1-)=Ir(C8H12)((C6H5)4Sb2(CH2)3)BF4 (912311-39-8)

Guidance literature:

In acetone; toluene; byproducts: AgCl; (under Ar or N2, Schlenk); Ir-complex and AgBF4 dissolved in acetone, heated gently for 30 min, filtered, added dropwise to soln. of Sb-compoundin toluene, stirred at room temp. for 30 min; vol. reduced, filtered, dried in vacuo; elem. anal.;

DOI:10.1039/b605198g

upstream raw materials:

silver tetrafluoroborate

bis(1,5-cyclooctadiene)diiridium(I) dichloride

1,3-bis(diphenylstibino)propane