Technology Process of C20H30OSi
There total 5 articles about C20H30OSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran
2: pyridinium chlorochromate / dichloromethane / 20 °C
3: potassium carbonate / methanol / 20 °C
4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 10 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; potassium carbonate; triethylamine; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201405215
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium chlorochromate / dichloromethane / 20 °C
2: potassium carbonate / methanol / 20 °C
3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 10 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; pyridinium chlorochromate;
In
methanol; dichloromethane;
DOI:10.1002/anie.201405215
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / methanol / 20 °C
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 10 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine;
In
methanol;
DOI:10.1002/anie.201405215
