2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL

Base Information

• Chemical Name: 2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL
• CAS No.: 20624-89-9
• Molecular Formula: C9H11 Cl O3
• Molecular Weight: 202.638
• Hs Code.: 2909499000
• Mol file: 20624-89-9.mol

Synonyms:Veratrylalcohol, 6-chloro- (6CI,8CI); (2-Chloro-4,5-dimethoxyphenyl)methanol

Chemical Property of 2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL

Chemical Property:

• Vapor Pressure: 0.000312mmHg at 25°C
• Melting Point: 70-72°C
• Boiling Point: 307.6°Cat760mmHg
• PKA: 13.77±0.10(Predicted)
• Flash Point: 139.8°C
• PSA: 38.69000
• Density: 1.241g/cm³
• LogP: 1.84950

Purity/Quality:

99% ^*data from raw suppliers

2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL

There total 2 articles about 2-CHLORO-3,4-DIMETHOXYBENZYL ALCOHOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-chloroverataldehyde (18093-05-5) → (2-chloro-4,5-dimethoxy-phenyl)-methanol (20624-89-9)

Guidance literature:

With sodium tetrahydroborate; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2012.07.010

Reference yield:

→ (2-chloro-4,5-dimethoxy-phenyl)-methanol (20624-89-9)

Guidance literature:

6-Chlor-3,4-dimethoxy-benzaldehyd, NaBH4, Me., Siedetemp.;

DOI:10.1021/jo01075a010

Reference yield:

(2-chloro-4,5-dimethoxy-phenyl)-methanol (20624-89-9) → 2-chloro-4,5-dimethoxybenzyl bromide (133230-10-1)

Guidance literature:

With phosphorus tribromide; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2012.07.010

upstream raw materials:

6-chloroverataldehyde

Downstream raw materials:

2-chloro-4,5-dimethoxybenzyl bromide

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