(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

Base Information

Chemical Name:(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester
CAS No.:562864-16-8
Molecular Formula:C₃₇H₅₆N₆O₈S
Molecular Weight:744.953
Hs Code.:

(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

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Chemical Property of (S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

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Technology Process of (S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

There total 16 articles about (S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 562864-23-7
C₄₂H₆₁Cl₃N₆O₁₀S

: 562864-16-8
(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: With Cd/Pb; ammonium acetate; In tetrahydrofuran; at 20 ℃; for 0.833333h;
DOI:10.1016/S0040-4020(03)00293-X

Reference yield:

: 260782-45-4
1-(2-{2-[(1-{2-[3-(1,1-dimethyl-allyloxy)-2-(4-nitro-benzyloxycarbonylamino)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

: 562864-16-8
(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: With zinc; In tetrahydrofuran; phosphate buffer; pH=6;
DOI:10.1016/S0040-4039(99)01955-3

Reference yield:

: 340270-70-4
(S)-3-(1,1-Dimethyl-allyloxy)-2-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-propionic acid

: 562864-16-8
(S)-1-((2S,3S)-2-{(S)-2-[((S)-1-{(S)-2-[(S)-2-Amino-3-(1,1-dimethyl-allyloxy)-propionylamino]-3-phenyl-propionyl}-pyrrolidine-2-carbothioyl)-amino]-3-hydroxy-propionylamino}-3-methyl-pentanoyl)-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 148 mg / diisopropylethylamine; HOBt; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 33 h / 0 - 20 °C

2: Cd/Pb; aq. NH₄OAc / tetrahydrofuran / 0.83 h / 20 °C

With Cd/Pb; ammonium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(03)00293-X