[RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

Base Information

Chemical Name:[RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]
CAS No.:1338249-99-2
Molecular Formula:C₂₁H₁₃Cl₃I₂N₃Ru
Molecular Weight:768.592
Hs Code.:

[RuCl<sub>3</sub>(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

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Technology Process of [RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

There total 1 articles about [RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 943895-68-9
4'-(3,5-diiodophenyl)-2,2':6',2-terpyridine

: 14898-67-0
ruthenium trichloride hydrate

: 1338249-99-2
[RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

Guidance literature:: In methanol; stirring soln. of terpyridine deriv. and ruthenium compd. in methanol, stirring at 25°C for 1 h, refluxing for 8 h; cooling to room temp., filtration, washing with methanol and CHCl3;
DOI:10.1039/c1nj20195f

Reference yield: 77.0%

: ammonium hexafluorophosphate

: 1338249-99-2
[RuCl₃(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)]

: 13104-56-8
2,6-bis(2'-pyridyl)-4-(p-methoxyphenyl)pyridine

: [Ru(II)(4'-(p-methoxyphenyl)-2,2':6',2''-terpyridine)(4'-(3,5-diiodophenyl)-2,2':6',2''-terpyridine)](PF₆)2

Guidance literature:: With N-ethylmorpholine; In methanol; addn. of morpholine deriv. to mixt. od ruthenium compd. and terpyridine deriv. in methanol, stirring at room temp. for 1 h, refluxing for 12 h; evapn. in vac., chromy. (SiO2, H2O/concd. aq. KNO3/CH3CN (1:1:10)), treatment with methanolic NH4PF6, isolation of ppt., NMR and MS;
DOI:10.1039/c1nj20195f