4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

Base Information

Chemical Name:4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone
CAS No.:1246766-87-9
Molecular Formula:C₃₀H₃₆O₄S₄
Molecular Weight:588.877
Hs Code.:

Synonyms:

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Chemical Property of 4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

Chemical Property:

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Technology Process of 4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

There total 1 articles about 4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₃₈O₄S₄

: 1225504-27-7
4,4'-sulfanediylbis(3,6-di-tert-butylcyclohexa-3,5-diene-1,2-dione)

: 1246766-87-9
4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

Guidance literature:: With oxygen; potassium carbonate; potassium hexacyanoferrate(III); In diethyl ether; water; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tet.2010.07.038

Reference yield:

: 1246766-87-9
4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

: 603-35-0
triphenylphosphine

: [Cu((C₆H₅)3P(CS₂C₆O₂(C(CH₃)3)2)2)(P(C₆H₅)3)2]

Guidance literature:: With Cu#Hg; In not given; reduction of di-o-quinone with copper amalgame in the presence of PPh3 in sealed tube; ESR spectroscopy;
DOI:10.1007/s11172-010-0299-5

Reference yield:

: 1246766-87-9
4,4',7,7'-tetra-tert-butyl-2,2'-bis-1,3-benzodithiol-5,5',6,6'-tetraone

: 603-36-1
triphenylantimony

: [Sb(C₆H₅)3((CS₂C₆O₂(C(CH₃)3)2)2)Sb(C₆H₅)3]⁽¹⁺⁾

Guidance literature:: With CuCl₂ or CF₃SO₃Ag or I₂; In tetrahydrofuran; according to V. K. Cherkasov, E. V. Grunova, G. A. Abakumov, Russ. Chem.Bull., Int. Ed., 2005, 54, 2067; small amt. of oxidizing agent added to soln. of dicatecholate prepd. in situ;
DOI:10.1007/s11172-010-0299-5