Bis(1-oxopyridin-2-thiolato)phenylbismut

Base Information

Chemical Name:Bis(1-oxopyridin-2-thiolato)phenylbismut
CAS No.:49771-43-9
Molecular Formula:C₁₆H₁₃BiN₂O₂S₂
Molecular Weight:538.404
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis(1-oxopyridin-2-thiolato)phenylbismut

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Technology Process of Bis(1-oxopyridin-2-thiolato)phenylbismut

There total 3 articles about Bis(1-oxopyridin-2-thiolato)phenylbismut which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 3811-73-2
2-mercaptopyridine-1-oxide sodium salt

: 4723-24-4
diphenylbismuth acetate

: 49771-43-9
Bis(1-oxopyridin-2-thiolato)phenylbismut

Guidance literature:: In N,N-dimethyl-formamide; ratio of educts 1:1; 15 minutes at 32 °C and 1.25 h at 65 °C, addn. of CH2Cl2 and H2O; crystn. of the product from the CH2Cl2 phase; soln. in N,N-dimethylacetamide and pptn. with water several times;
DOI:10.1039/DT9720001120