7-Methoxy-1-methylindolin-2-one

Base Information

Chemical Name:7-Methoxy-1-methylindolin-2-one
CAS No.:7699-23-2
Molecular Formula:C₁₀H₁₁NO₂
Molecular Weight:177.203
Hs Code.:
DSSTox Substance ID:DTXSID401255026
Nikkaji Number:J1.971.492F

Synonyms:7-Methoxy-1-methylindolin-2-one;7699-23-2;SCHEMBL8999207;DTXSID401255026;1,3-dihydro-7-methoxy-1-methyl-2H-Indol-2-one

Suppliers and Price of 7-Methoxy-1-methylindolin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 7-Methoxy-1-methylindolin-2-one

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:177.078978594
Heavy Atom Count:13
Complexity:217

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=O)CC2=C1C(=CC=C2)OC

Technology Process of 7-Methoxy-1-methylindolin-2-one

There total 2 articles about 7-Methoxy-1-methylindolin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21744-84-3
4-methyl-4H-benzo[1,4]oxazin-3-one

: 7699-21-0
4-methoxy-1-methyloxindole

: 7699-23-2
7-methoxy-1-methylindolin-2-one

Guidance literature:: With aluminium trichloride; at 220 ℃; Behandeln des Reaktionsprodukts mit Dimethylsulfat und wss.Natronlauge;

Reference yield:

: 77747-62-7
N-chloroacetyl-N-methyl-o-anisidine

: 7699-21-0
4-methoxy-1-methyloxindole

: 7699-23-2
7-methoxy-1-methylindolin-2-one

Guidance literature:: With aluminium trichloride; at 220 ℃; Erwaermen des Reaktionsprodukts mit Methyljodid und Kaliumcarbonat in Aceton;
DOI:10.1039/jr9550000739

Reference yield:

: 7699-23-2
7-methoxy-1-methylindolin-2-one

: 1025908-15-9
7-Methoxy-1-methyl-2-thioxo-2,3-dihydro-1H-indole-3-carboxylic acid phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Na₂CO₃, P₂S₅ / tetrahydrofuran / Ambient temperature

2: 1.) NaH / 1.) THF, 2.) THF

With tetraphosphorus decasulfide; sodium hydride; sodium carbonate; In tetrahydrofuran;
DOI:10.1021/jm00039a016