C₂₄H₂₆N₂O₃

Base Information

• Chemical Name: C₂₄H₂₆N₂O₃
• CAS No.: 1448802-16-1
• Molecular Formula: C₂₄H₂₆N₂O₃
• Molecular Weight: 390.482

Synonyms:

Chemical Property of C₂₄H₂₆N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₂₄H₂₆N₂O₃

There total 12 articles about C₂₄H₂₆N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

C24H26N2O3 → C24H26N2O3 (1448802-15-0) + C24H26N2O3 (1448802-16-1)

Guidance literature:

With Daicel Chiral-Pak AS; In ethanol; hexane; diethylamine; Resolution of racemate;

DOI:10.1002/anie.201208297

Reference yield:

C36H35N2O6P + methylmagnesium chloride (676-58-4) → C24H26N2O3 (1448802-16-1)

Guidance literature:

C₃₆H₃₅N₂O₆P; With copper(l) iodide; In tetrahydrofuran; at 0 ℃; for 0.25h;

methylmagnesium chloride; at 0 - 20 ℃; for 0.583333h; Further stages;

DOI:10.1002/chem.201604647

Reference yield:

C40H46N2O5 → C24H26N2O3 (1448802-16-1)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

1.2: 0.83 h

1.3: 6.5 h

2.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1 h / 110 °C

3.1: diisobutylaluminium hydride / dichloromethane / 0.17 h / -78 °C

4.1: triethylamine; dmap / dichloromethane / 1 h / 0 - 20 °C

5.1: copper(l) iodide / tetrahydrofuran / 0.25 h / 0 °C

5.2: 0.58 h / 0 - 20 °C

With dmap; copper(l) iodide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

DOI:10.1002/chem.201604647

upstream raw materials:

methylmagnesium chloride

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