C₁₈H₂₅N₅O₆

Base Information

Chemical Name:C₁₈H₂₅N₅O₆
CAS No.:1449145-46-3
Molecular Formula:C₁₈H₂₅N₅O₆
Molecular Weight:407.426
Hs Code.:

C<sub>18</sub>H<sub>25</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₅N₅O₆

Chemical Property:

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Technology Process of C₁₈H₂₅N₅O₆

There total 7 articles about C₁₈H₂₅N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449145-45-2
C₁₉H₂₆N₄O₇

: 1449145-46-3
C₁₈H₂₅N₅O₆

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at -10 ℃; for 4h;
DOI:10.1002/anie.201206968

Reference yield:

: 1449145-44-1
C₁₃H₁₆N₂O₅

: 1449145-46-3
C₁₈H₂₅N₅O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium bicarbonate; di-tert-butyl dicarbonate; pyridine / acetonitrile / 6 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / -10 °C

2.2: 9 h / -10 - 20 °C / Inert atmosphere

With pyridine; di-tert-butyl dicarbonate; palladium 10% on activated carbon; hydrogen; ammonium bicarbonate; In methanol; acetonitrile;
DOI:10.1002/anie.201206968

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1449145-46-3
C₁₈H₂₅N₅O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0.17 h / -10 °C / Inert atmosphere

1.2: 6 h / -10 - 20 °C / Inert atmosphere

2.1: methylmagnesium bromide / tetrahydrofuran; diethyl ether / 3 h / 20 °C / Inert atmosphere

2.2: 20 °C

3.1: sodium hydroxide / water / 1 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / -10 °C

4.2: 9 h / -10 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; methylmagnesium bromide; hydrogen; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/anie.201206968