ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

Base Information

Chemical Name:ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate
CAS No.:1253736-31-0
Molecular Formula:C₁₉H₁₈BrNO₆
Molecular Weight:436.259
Hs Code.:

Synonyms:

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Chemical Property of ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

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Technology Process of ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

There total 4 articles about ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1253736-31-0
ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium hydrobromide perbromide / methanol / 3 h / 20 °C

2: diethyl amine hydrochloride / toluene / 72 h / Dean-Stark; Reflux; Inert atmosphere

With diethyl amine hydrochloride; pyridinium hydrobromide perbromide; In methanol; toluene;
DOI:10.1002/asia.201500611

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1253736-31-0
ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / ethanol / 6 h / Reflux

2: pyridinium hydrobromide perbromide / methanol / 3 h / 20 °C

3: diethyl amine hydrochloride / toluene / 72 h / Dean-Stark; Reflux; Inert atmosphere

With diethyl amine hydrochloride; potassium carbonate; pyridinium hydrobromide perbromide; In methanol; ethanol; toluene;
DOI:10.1002/asia.201500611

Reference yield:

: 100-39-0
benzyl bromide

: 1253736-31-0
ethyl 3-[4-(benzyloxy)-2-bromo-5-methoxyphenyl]-2-nitroacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / ethanol / 6 h / Reflux

2: pyridinium hydrobromide perbromide / methanol / 3 h / 20 °C

3: diethyl amine hydrochloride / toluene / 72 h / Dean-Stark; Reflux; Inert atmosphere

With diethyl amine hydrochloride; potassium carbonate; pyridinium hydrobromide perbromide; In methanol; ethanol; toluene;
DOI:10.1002/asia.201500611