C₃₉H₆₀N₇O₆PSi

Base Information

• Chemical Name: C₃₉H₆₀N₇O₆PSi
• CAS No.: 1332889-28-7
• Molecular Formula: C₃₉H₆₀N₇O₆PSi
• Molecular Weight: 782.008
• Mol file: 1332889-28-7.mol

Synonyms:

Chemical Property of C₃₉H₆₀N₇O₆PSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₆₀N₇O₆PSi

There total 3 articles about C₃₉H₆₀N₇O₆PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-azidopropyltriethoxysilane (83315-69-9) + tris(methoxybenzyl)proazaphosphatrane (1267779-24-7) → C39H60N7O6PSi (1332889-28-7)

Guidance literature:

In toluene; at 60 ℃; for 72h; Inert atmosphere;

DOI:10.1002/adsc.201100270

Reference yield:

tris(4-methoxybenzyl)tren → C39H60N7O6PSi (1332889-28-7)

Guidance literature:

Multi-step reaction with 3 steps

1: bis(N,N-dimethylamino)chlorophosphine / acetonitrile / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / Inert atmosphere

3: toluene / 72 h / 60 °C / Inert atmosphere

With bis(N,N-dimethylamino)chlorophosphine; potassium tert-butylate; In tetrahydrofuran; toluene; acetonitrile;

DOI:10.1002/adsc.201100270

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → C39H60N7O6PSi (1332889-28-7)

Guidance literature:

Multi-step reaction with 5 steps

1: isopropyl alcohol / Inert atmosphere

2: sodium tetrahydroborate / methanol / Inert atmosphere

3: bis(N,N-dimethylamino)chlorophosphine / acetonitrile / Inert atmosphere

4: potassium tert-butylate / tetrahydrofuran / Inert atmosphere

5: toluene / 72 h / 60 °C / Inert atmosphere

With sodium tetrahydroborate; bis(N,N-dimethylamino)chlorophosphine; potassium tert-butylate; In tetrahydrofuran; methanol; isopropyl alcohol; toluene; acetonitrile;

DOI:10.1002/adsc.201100270

upstream raw materials:

3-azidopropyltriethoxysilane

tris(methoxybenzyl)proazaphosphatrane

4-methoxy-benzaldehyde

Refernces

• 1、 Raytchev, Pascal Dimitrov,Roussi, Lyvie,Dutasta, Jean-Pierre,Martinez, Alexandre,Dufaud, Véronique. "Homogeneous and silica-supported azidoproazaphosphatranes as efficient catalysts for the synthesis of substituted coumarins". . p. 1 - 4. Retrieved 2012.