C₃₆H₄₃Cl₃N₂O₆S

Base Information

Chemical Name:C₃₆H₄₃Cl₃N₂O₆S
CAS No.:1374451-20-3
Molecular Formula:C₃₆H₄₃Cl₃N₂O₆S
Molecular Weight:738.172
Hs Code.:

C<sub>36</sub>H<sub>43</sub>Cl<sub>3</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₃₆H₄₃Cl₃N₂O₆S

Chemical Property:

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Technology Process of C₃₆H₄₃Cl₃N₂O₆S

There total 4 articles about C₃₆H₄₃Cl₃N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115-20-8
1,1,1-trichloroethanol

: C₃₄H₄₂N₂O₆S

: 1374451-20-3
C₃₆H₄₃Cl₃N₂O₆S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290339

Reference yield:

: C₈H₁₇NO₃

: 1374451-20-3
C₃₆H₄₃Cl₃N₂O₆S

Guidance literature:: Multi-step reaction with 3 steps

1: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2: sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With dmap; (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-0031-1290339

Reference yield:

: 22838-58-0
Boc-D-Val-OH

: 1374451-20-3
C₃₆H₄₃Cl₃N₂O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 0 °C / Inert atmosphere

1.2: 45 °C / Inert atmosphere

2.1: potassium borohydride / methanol / 1.5 h / -78 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

4.1: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

5.1: sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With dmap; potassium borohydride; (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1055/s-0031-1290339