5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

Base Information

Chemical Name:5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine
CAS No.:82137-51-7
Molecular Formula:C₁₆H₂₀N₄O₂Si
Molecular Weight:328.446
Hs Code.:

Synonyms:

Suppliers and Price of 5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

Chemical Property:

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Technology Process of 5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

There total 7 articles about 5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 82137-51-7
5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

Guidance literature:: Multi-step reaction with 6 steps

1: 58 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 2 h

2: 93 percent / NaNO₂ / H₂O; dimethylformamide / 24 h / 80 - 90 °C

3: 80 percent / methanolic ammonia / dimethylformamide / 22 h / 130 °C / a sealed, glass-lined steel bomb

4: 85 percent / H₂ / PtO₂ / ethanol; ethyl acetate / 0.5 h / 1520 Torr / Ambient temperature

5: acetic anhydride / 1 h / Heating

6: amonium sulfate / Heating

With ammonium sulfate; ammonia; hydrogen; acetic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium nitrite; platinum(IV) oxide; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210243

Reference yield:

: 92574-75-9
2-((benzyloxy)methyl)-4,5-dichloropyridazin-3(2H)-one

: 82137-51-7
5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / NaNO₂ / H₂O; dimethylformamide / 24 h / 80 - 90 °C

2: 80 percent / methanolic ammonia / dimethylformamide / 22 h / 130 °C / a sealed, glass-lined steel bomb

3: 85 percent / H₂ / PtO₂ / ethanol; ethyl acetate / 0.5 h / 1520 Torr / Ambient temperature

4: acetic anhydride / 1 h / Heating

5: amonium sulfate / Heating

With ammonium sulfate; ammonia; hydrogen; acetic anhydride; sodium nitrite; platinum(IV) oxide; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210243

Reference yield:

: 92574-76-0
4-hydroxy-5-nitro-2-benzyloxymethylpyridazin-3-one

: 82137-51-7
5-Benzyloxymethyl-4-trimethylsilanyloxy-5H-imidazo[4,5-d]pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / methanolic ammonia / dimethylformamide / 22 h / 130 °C / a sealed, glass-lined steel bomb

2: 85 percent / H₂ / PtO₂ / ethanol; ethyl acetate / 0.5 h / 1520 Torr / Ambient temperature

3: acetic anhydride / 1 h / Heating

4: amonium sulfate / Heating

With ammonium sulfate; ammonia; hydrogen; acetic anhydride; platinum(IV) oxide; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210243