C₄₂H₅₁N₅O₂

Base Information

Chemical Name:C₄₂H₅₁N₅O₂
CAS No.:1422268-73-2
Molecular Formula:C₄₂H₅₁N₅O₂
Molecular Weight:657.899
Hs Code.:

C<sub>42</sub>H<sub>51</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₂H₅₁N₅O₂

Chemical Property:

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Technology Process of C₄₂H₅₁N₅O₂

There total 4 articles about C₄₂H₅₁N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422268-67-4
C₃₄H₃₇BrN₄

: 78888-18-3
N-tert-butoxycarbonylprop-2-en-1-amine

: 1422268-73-2
C₄₂H₅₁N₅O₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; palladium dichloride; In N,N-dimethyl-formamide; at 120 ℃; for 8h;
DOI:10.1021/jm4000984

Reference yield:

: 35510-04-4
1-bromo-2,4-bis(bromomethyl)benzene

: 1422268-73-2
C₄₂H₅₁N₅O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 0.17 h / 0 °C

2.1: palladium dichloride; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 8 h / 120 °C

With n-butyllithium; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; palladium dichloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 2.1: |Heck Reaction;
DOI:10.1021/jm4000984

Reference yield:

: 6939-93-1
4-bromo-isophthalic acid

: 1422268-73-2
C₄₂H₅₁N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2.1: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.2: 0.17 h / 0 °C

4.1: palladium dichloride; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 8 h / 120 °C

With lithium borohydride; n-butyllithium; chloro-trimethyl-silane; carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; tris-(o-tolyl)phosphine; palladium dichloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 4.1: |Heck Reaction;
DOI:10.1021/jm4000984