Technology Process of C20H19NO2
There total 4 articles about C20H19NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
8-Methoxy-1,2,3,9-tetrahydro-carbazol-4-one;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 2h;
benzyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/jo402741g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C
2.2: 2 h / 0 - 20 °C
With
copper diacetate; palladium diacetate; sodium hydride; potassium carbonate;
In
N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo402741g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / toluene
2.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C
3.2: 2 h / 0 - 20 °C
With
copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid;
In
N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jo402741g
