trans-N-(2,2-Dimethylpropylidene)-o-aminophenol

Base Information

• Chemical Name: trans-N-(2,2-Dimethylpropylidene)-o-aminophenol
• CAS No.: 70299-35-3
• Molecular Formula: C₁₁H₁₅NO
• Molecular Weight: 177.246

Synonyms:

Chemical Property of trans-N-(2,2-Dimethylpropylidene)-o-aminophenol

Chemical Property:

Purity/Quality:

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Technology Process of trans-N-(2,2-Dimethylpropylidene)-o-aminophenol

There total 2 articles about trans-N-(2,2-Dimethylpropylidene)-o-aminophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

pivalaldehyde (630-19-3) + 2-amino-phenol (95-55-6) → trans-N-(2,2-Dimethylpropylidene)-o-aminophenol (70299-35-3)

Guidance literature:

In Cyclopentane; Heating;

DOI:10.1021/jo00334a029

Reference yield:

trans-N-(2,2-Dimethylpropylidene)-o-aminophenol (70299-35-3) → 2-tert-butyl-1,3-benzoxazole (54696-03-6) + 2-tert-Butyl-2,3-dihydro-benzooxazole + cis-N-(2,2-Dimethylpropylidene)-o-aminophenol (70299-35-3)

Guidance literature:

In methyl cyclohexane; Title compound not separated from byproducts; Ambient temperature; Irradiation;

DOI:10.1021/jo00334a029

Reference yield:

trans-N-(2,2-Dimethylpropylidene)-o-aminophenol (70299-35-3) → 2-tert-butyl-1,3-benzoxazole (54696-03-6) + 2-tert-Butyl-2,3-dihydro-benzooxazole + cis-N-(2,2-Dimethylpropylidene)-o-aminophenol (70299-35-3)

Guidance literature:

In methyl cyclohexane; Title compound not separated from byproducts; Ambient temperature; Irradiation;

DOI:10.1021/jo00334a029

upstream raw materials:

pivalaldehyde

2-amino-phenol

Downstream raw materials:

2-tert-butyl-1,3-benzoxazole

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