2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

Base Information

Chemical Name:2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal
CAS No.:125353-72-2
Molecular Formula:C₂₆H₃₂O₂
Molecular Weight:376.539
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

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Technology Process of 2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

There total 3 articles about 2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3360-41-6
4-phenyl-butan-1-ol

: 125353-72-2
2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / pyridinium dichromate / CH₂Cl₂ / 10 h / Ambient temperature

2: 27 percent / a) HgCl₂, Mg, b) TiCl₄ / tetrahydrofuran / 24 h / 0 °C

3: 1.) BF₃*Et₂O or p-toluenesulfonic acid monohydrate, 2.) NaOMe / 1.) CH₂Cl₂, 0 deg C, 2.) DMSO, room temperature

With dipyridinium dichromate; boron trifluoride diethyl etherate; sodium methylate; titanium tetrachloride; magnesium; mercury dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00294a016

Reference yield:

: 18328-11-5
3-benzyl propionaldehyde

: 125353-72-2
2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / a) HgCl₂, Mg, b) TiCl₄ / tetrahydrofuran / 24 h / 0 °C

2: 1.) BF₃*Et₂O or p-toluenesulfonic acid monohydrate, 2.) NaOMe / 1.) CH₂Cl₂, 0 deg C, 2.) DMSO, room temperature

With boron trifluoride diethyl etherate; sodium methylate; titanium tetrachloride; magnesium; mercury dichloride; In tetrahydrofuran;
DOI:10.1021/jo00294a016

Reference yield:

: 1728-36-5
3-Brom-2-methoxy-1-cyclohexen

: 22632-23-1
(dl)-1,8-diphenyl-4,5-octanediol

: 125353-72-2
2-cyclohexen-1-one 1,8-diphenyl-4,5-octanediol ketal

Guidance literature:: With boron trifluoride diethyl etherate; sodium methylate; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 2.) DMSO, room temperature;
DOI:10.1021/jo00294a016