(ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II)

Base Information

Chemical Name:(ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II)
CAS No.:771488-45-0
Molecular Formula:C₃₄H₃₂N₄Ni₂O₆S₄
Molecular Weight:838.295
Hs Code.:

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Chemical Property of (ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II)

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Technology Process of (ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II)

There total 1 articles about (ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3232-37-9,71112-98-6
salicylaldehyde benzoylhydrazone

: 140-89-6
potassium ethyl xanthogenate

: 83864-14-6
nickel dichloride

: 771488-45-0
(ethyl dithiocarbonate)(salicylaldehyde benzoylhydrazone anion)nickel(II)

Guidance literature:: In ethanol; water; byproducts: KCl, HCl; salicylaldehyde benzoylhydrazone (1 equiv.) dissolved in abs. EtOH; added to NiCl2 in aq. EtOH; stirred for ca. 0.5 h; K alkyl dithiocarbonate (1 equiv.) in doubly distd. water added with stirring; filtered; ppt. washed with aq. EtOH; dried over P2O5; elem. anal.;
DOI:10.1081/SIM-120035954