diphenyl <1--3-methylbutyl>phosphonate

Base Information

• Chemical Name: diphenyl <1--3-methylbutyl>phosphonate
• CAS No.: 90763-52-3
• Molecular Formula: C₂₅H₂₈NO₅P
• Molecular Weight: 453.475

Synonyms:

Chemical Property of diphenyl <1--3-methylbutyl>phosphonate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Useful:

Technology Process of diphenyl <1--3-methylbutyl>phosphonate

There total 1 articles about diphenyl <1--3-methylbutyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

triphenyl phosphite (101-02-0) + O-benzyl carbamate (621-84-1) + isovaleraldehyde (590-86-3) → diphenyl <1--3-methylbutyl>phosphonate (90763-52-3,125882-52-2,125882-59-9,73270-45-8)

Guidance literature:

With acetic acid; at 80 ℃; for 1h;

DOI:10.1080/10426509808045494

Reference yield: 100.0%

methanol (67-56-1) + diphenyl <1--3-methylbutyl>phosphonate (90763-52-3,125882-52-2,125882-59-9,73270-45-8) → dimethyl {1-[(benzyloxycarbonyl)amino]-3-methylbutyl}phosphonate (82629-28-5)

Guidance literature:

With sodium methylate; at 22 ℃; for 2h;

DOI:10.1021/jm00392a014

Reference yield: 96.0%

diphenyl <1--3-methylbutyl>phosphonate (90763-52-3,125882-52-2,125882-59-9,73270-45-8) → diphenyl (1-amino-3-methyl)butylphosphonate (73270-43-6)

Guidance literature:

With hydrogen bromide; In acetic acid; at 22 ℃; for 1h;

DOI:10.1021/jm00392a014

upstream raw materials:

triphenyl phosphite

O-benzyl carbamate

isovaleraldehyde

Downstream raw materials:

dimethyl {1-[(benzyloxycarbonyl)amino]-3-methylbutyl}phosphonate

methyl <1--3-methylbutyl>phosphonate

(1-Benzyloxycarbonylamino-3-methyl-butyl)-phosphonic acid dipropyl ester

(1-Benzyloxycarbonylamino-3-methyl-butyl)-phosphonic acid monoethyl ester

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