3-isopropoxy-2-isopropylbenzamide

Base Information

Chemical Name:3-isopropoxy-2-isopropylbenzamide
CAS No.:1369910-08-6
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:

Synonyms:

Suppliers and Price of 3-isopropoxy-2-isopropylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-isopropoxy-2-isopropylbenzamide

Chemical Property:

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Technology Process of 3-isopropoxy-2-isopropylbenzamide

There total 4 articles about 3-isopropoxy-2-isopropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369819-67-9
3-isopropoxy-2-isopropylbenzonitrile

: 1369910-08-6
3-isopropoxy-2-isopropylbenzamide

Guidance literature:: With dihydrogen peroxide; potassium carbonate; In dimethyl sulfoxide; at 0 - 20 ℃; for 24h;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775

Reference yield:

2,3-dimethoxybenzonitrile: 5653-62-3
2,3-dimethoxybenzonitrile

: 1369910-08-6
3-isopropoxy-2-isopropylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: aluminum tri-bromide; 1-thiopropane / dichloromethane / 0 - 20 °C / Inert atmosphere

3: caesium carbonate / acetonitrile / 24 h / 20 °C / Inert atmosphere

4: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 24 h / 0 - 20 °C

With aluminum tri-bromide; 1-thiopropane; dihydrogen peroxide; potassium carbonate; caesium carbonate; In diethyl ether; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775

Reference yield:

: 1243279-74-4
3-hydroxy-2-isopropylbenzonitrile

: 1369910-08-6
3-isopropoxy-2-isopropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 24 h / 20 °C / Inert atmosphere

2: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 24 h / 0 - 20 °C

With dihydrogen peroxide; potassium carbonate; caesium carbonate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775