(E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

Base Information

Chemical Name:(E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester
CAS No.:134224-10-5
Molecular Formula:C₈₀H₉₅NO₁₀
Molecular Weight:1230.63
Hs Code.:

(E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

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Chemical Property of (E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

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Technology Process of (E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

There total 3 articles about (E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16331-52-5
9-anthracenecarbonyl chloride

: 134224-10-5
(E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / tetrahydrofuran / 1 h / Ambient temperature

2: 64 percent / Et₃N / dimethylformamide / 2 h / 60 °C

3: Et₃N, DMAP / CH₂Cl₂

With dmap; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39910000256

Reference yield:

: 133870-79-8
9-anthroyl tetrazole

: 134224-10-5
(E)-3-(4-Methoxy-phenyl)-acrylic acid (R)-1-{(1R,2S)-3-[(anthracene-9-carbonyl)-amino]-1,2-bis-[(E)-3-(4-methoxy-phenyl)-acryloyloxy]-propyl}-4-((3R,5bR,11aS)-hexamethyl-icosahydro-cyclopenta[a]chrysen-3-yl)-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / Et₃N / dimethylformamide / 2 h / 60 °C

2: Et₃N, DMAP / CH₂Cl₂

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39910000256