C₂₂H₂₀OS₂

Base Information

Chemical Name:C₂₂H₂₀OS₂
CAS No.:1443988-19-9
Molecular Formula:C₂₂H₂₀OS₂
Molecular Weight:364.532
Hs Code.:

C<sub>22</sub>H<sub>20</sub>OS<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₀OS₂

Chemical Property:

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Technology Process of C₂₂H₂₀OS₂

There total 5 articles about C₂₂H₂₀OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432518-88-1
2-[bis(phenylsulfanyl)methyl]benzaldehyde

: 4009-98-7
(methoxymethyl)triphenylphosphonium chloride

: 1443988-19-9
C₂₂H₂₀OS₂

Guidance literature:: (methoxymethyl)triphenylphosphonium chloride; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1.5h;

2-[bis(phenylsulfanyl)methyl]benzaldehyde; In tetrahydrofuran; for 12h; Cooling with ice;
DOI:10.1039/c3ob40115d

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 1443988-19-9
C₂₂H₂₀OS₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromine / tetrachloromethane / Irradiation

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 12 h

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.33 h / -78 °C / Cooling with ice

4.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 12 h / 0 °C / Cooling with ice

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -78 °C

5.2: 12 h / Cooling with ice

With bromine; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 5.1: |Wittig Olefination;
DOI:10.1039/c3ob40115d

Reference yield:

: 1432518-92-7
{2-[bis(phenylsulfanyl)methyl]phenyl}methanol

: 1443988-19-9
C₂₂H₂₀OS₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 12 h / 0 °C / Cooling with ice

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -78 °C

2.2: 12 h / Cooling with ice

With sodium hexamethyldisilazane; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 2.1: |Wittig Olefination;
DOI:10.1039/c3ob40115d