C₃₃H₂₉NO₆*C₇H₅N

Base Information

• Chemical Name: C₃₃H₂₉NO₆*C₇H₅N
• CAS No.: 131354-99-9
• Molecular Formula: C₇H₅N*C₃₃H₂₉NO₆
• Molecular Weight: 638.72
• Mol file: 131354-99-9.mol

Synonyms:

Chemical Property of C₃₃H₂₉NO₆*C₇H₅N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₂₉NO₆*C₇H₅N

There total 8 articles about C₃₃H₂₉NO₆*C₇H₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dibromonaphthalene (13214-70-5) → C33H29NO6*C7H5N (131354-99-9)

Guidance literature:

Multi-step reaction with 6 steps

1: 35.8 percent / CuO₂, 1,3-dimethylimidazolin-2-one / 46 h / 170 - 180 °C

2: 97 percent / BBr₃ / CH₂Cl₂ / 3 h / 0 °C

3: 1.) Cs₂CO₃ / 1.) DMF, 80 deg C, 1 h, 2.) 80 deg C, 6 h

4: 82 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 25 °C / 2280 Torr

5: 52 percent / NaH / tetrahydrofuran / 4 h / Heating

6: 12 h / Ambient temperature

With 1,3-dimethyl-2-imidazolinone; hydrogen; boron tribromide; sodium hydride; caesium carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;

DOI:10.1021/jo00003a055

Reference yield:

C22H16O4 (131354-69-3) → C33H29NO6*C7H5N (131354-99-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Cs₂CO₃ / 1.) DMF, 80 deg C, 1 h, 2.) 80 deg C, 6 h

2: 82 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 25 °C / 2280 Torr

3: 52 percent / NaH / tetrahydrofuran / 4 h / Heating

4: 12 h / Ambient temperature

With hydrogen; sodium hydride; caesium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;

DOI:10.1021/jo00003a055

Reference yield:

2,2'-(2,3-Naphthylenedioxy)diphenol bis(methyl ether) (131354-68-2) → C33H29NO6*C7H5N (131354-99-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 97 percent / BBr₃ / CH₂Cl₂ / 3 h / 0 °C

2: 1.) Cs₂CO₃ / 1.) DMF, 80 deg C, 1 h, 2.) 80 deg C, 6 h

3: 82 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 25 °C / 2280 Torr

4: 52 percent / NaH / tetrahydrofuran / 4 h / Heating

5: 12 h / Ambient temperature

With hydrogen; boron tribromide; sodium hydride; caesium carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;

DOI:10.1021/jo00003a055

upstream raw materials:

C₃₃H₂₉NO₆

benzonitrile

2,6-bis(chloromethyl)pyridine

2,3-dibromonaphthalene